Life Sciences

Terahertz imaging finds new applications

Terahertz imaging is experiencing a surge of interest for applications ranging from airport screening to chemical detection.
Oct. 1, 2003
12 min read

Terahertz imaging is experiencing a surge of interest for applications ranging from airport screening to chemical detection.

By Kathy Kincade

While microwave and x-ray technologies still make up the majority of imaging systems used for security applications, another part of the electromagnetic spectrum, terahertz frequencies, is now beginning to be used for both structural imaging and spectroscopy. The terahertz region encompasses frequencies between microwave and infrared, in the range of 100 GHz to 30 THz. Over the past decade, research in this part of the spectrum has been hampered by a lack of adequate sources and detectors, but recent advances in these areas have led to the development of a new generation of terahertz imagers that are making the technology more practical.

Much of the initial research in terahertz imaging took place in the early 1990s at AT&T Bell Labs (Holmdel, NJ, USA) under the direction of Binbin Hu and Martin Nuss. The resulting technology, based on optoelectronic terahertz time-domain spectroscopy, was licensed to Picometrix (Ann Arbor, MI, USA) in 1998; one year later, Picometrix introduced the first commercially available terahertz imager.

With the growing desire to better detect and monitor terrorist activities, the emphasis in many terahertz circles has shifted to security applications. The goal is to leverage the inherent advantages of terahertz waves-most notably the ability to image inside dielectric materials such as cloth, leather, plastic, cardboard, and common packaging materials and distinguish different chemical compositions inside those materials (see Fig. 1).

FIGURE 1. Terahertz waves penetrate dielectric materials such as cloth, leather, plastic, cardboard, thin walls, and common packaging materials and provide spectroscopic information. The visible image shows a razor blade obscured by two layers of denim material (left). With a terahertz imager, the entire razor blade can be detected clearly (right).

Click here to enlarge image

While microwave and x-ray imagers produce density pictures, terahertz rays go a step further, providing spectroscopic information within the terahertz frequency range. Certain parts of the terahertz spectrum also lend themselves to remote sensing of unknown gas clouds and airborne biohazards.

"Spectral information is the power of the terahertz regime," says Chris Mann, project manager for the StarTiger terahertz development program sponsored last year by the European Space Agency (ESA; Paris, France). "Everything has a spectral signature, and all materials emit terahertz waves, each having its own frequency pattern as a kind of fingerprint," he adds.

Applications near and far

Terahertz imaging systems are now under development for applications such as powder detection, screening for concealed weapons, and biological-agent analysis. Although remote terahertz imaging at frequencies below 0.5 THz is possible up to a few kilometers, use of frequencies above approximately 0.5 THz is primarily limited to short-distance spectroscopic applications, such as biological-agent and soil analysis, and should eventually find a place in whole-body imagers, once the technology becomes more compact and less expensive.

"Terahertz radiation does not penetrate very far into the atmosphere, although there are windows in the atmospheric spectrum where terahertz radiation does propagate a reasonable distance," said Mark Sherwin, professor of physics at the University of California, Santa Barbara (UCSB; Santa Barbara, CA, USA), who oversees several terahertz projects at the university. "If you are looking through someone's clothes a few feet away, there are windows of transparency at 2.5 and 1.6 THz and a fairly wide window at about 3 THz."

TeraView (Cambridge, England), a spinoff of Toshiba Europe's Research Laboratory, originally targeted its core technology at medical and dental applications but is now looking to adapt its terahertz platform for security applications, including postal inspection, object detection, chemical and bioagent detection, and landmine detection. The system contains a femtosecond diode-pumped Ti:sapphire laser oscillator tunable in the 750- to 890-nm range, a terahertz generator, coupling optics for the terahertz beam, and time-resolved electro-optical sampling.

"We have a development-stage product that uses the lower-frequency portion of the spectrum and can be configured for various applications," says Don Arnone, president of TeraView. "We are now looking at using this platform and developing a user interface for a security screening probe, initially as a second-stage screening device."

Similarly, technology originally developed at the Center for Terahertz Research at Rensselaer Polytechnic Institute (RPI; Troy, NY, USA) for biomedical applications is being investigated for other short-range spectroscopic applications such as the detection of explosive materials and bioagents. In a test, the group's 0.3-THz chirped-probe-beam terahertz imaging system scanned a postal envelope in two dimensions, distinguishing between 80-mg samples of flour, salt, baking soda, and seasoning.

To more accurately assess the applicability of terahertz imaging to anthrax detection, the researchers also considered samples of bacillus thurengiensis bacteria spores. Xi-Cheng Zhang of RPI uses the Fourier transform of the terahertz waveform to provide information on the frequency-dependent scattering, absorption, and refractive index of each sample. This technology is being commercialized through a startup company.

Basic science

Several research groups are working to overcome the technical issues that are likely to delay the introduction of commercial terahertz systems for another year or two. These limitations include water absorption and related signal-to-noise ratios, long data-acquisition times (tens of minutes to hours for a single image), lack of terahertz-specific optical components, and limited source power for large-scale imaging (except for free-electron lasers).

As part of the European Teravision program, for example, researchers at Delft University of Technology (Delft, The Netherlands) have built terahertz sources and detectors based on Ti:sapphire femtosecond laser oscillators and have developed a terahertz generation and detection scheme with the highest dynamic range in the world for these oscillators, according to Paul Planken, professor of applied sciences at Delft. By using lock-in detection at 50 kHz, they can measure the terahertz signal at a modulation frequency at which the laser noise is minimal.

"We currently measure a full 35-ps-long terahertz electric field with a dynamic range of more than 5000 in a total measurement time of 20 ms," he said. Planken and his colleagues have also developed a new method to overcome the diffraction limit in terahertz imaging and have improved the resolution of terahertz imaging by a factor of almost 1000.

Free-electron lasers are being used to demonstrate high-power terahertz capabilities and speed materials research. At Thomas Jefferson National Accelerator Facility (JLab; Newport News, VA, USA), researchers have generated terahertz rays at nearly 20-W average power—20,000 times stronger than previous attempts. In an experiment conducted in November 2001 by Gwyn Williams, scientists from JLab, Brookhaven National Laboratory (Upton, NY, USA), and Lawrence Berkeley National Laboratory (Berkeley, CA, USA) produced high-average-power broadband emission from 500-fs electron bunches in the JLab free electron laser (FEL) Superconducting Radio-Frequency (SRF) accelerator. Williams and George Neil, the FEL facility manager at JLab, have formed a company called Reletec to license some of the findings from the T-ray experiments for use in large imaging systems, such as the measurements of the terahertz response of potentially dangerous materials and imaging plastic explosives in nonmetallic dry structures.

Similarly, researchers at the Center for Terahertz Science and Technology at UCSB are working with two FELs to do materials research and proof of science in the 0.12- to 5-THz range, with peak powers of 1 kW. Through their research, they have developed a new detector, TACIT (tunable antenna-coupled intersubband terahertz), that could be used for security applications, much like a tiny spectrometer on a chip. They are also looking at terahertz detection of bioagents.

Optical vs. electronic sources

FIGURE 2. Terahertz system developed at the University of Wisconsin uses a broadband bowtie antenna integrated with an integrated electronic circuit called a nonlinear transmission line and sampling detector to generate short pulses in the 0.1- to 10-THz range.

Click here to enlarge image

The current size, cost, and field-deployability limitations of most terahertz imagers have prompted other research groups to focus on electronic sources for terahertz-wave generation, as opposed to the more popular optical methods (illuminating a semiconductor crystal, such as gallium arsenide, with femtosecond pulses of visible light). Daniel van der Weide and colleagues at the University of Wisconsin (Madison, WI, USA) are developing a compact terahertz system that uses electronic circuits to produce short pulses in the 0.1- to 10-THz range for remote imaging, and they are looking to commercialize this technology through a spin-off company (see Fig. 2). "Although laboratory results from optoelectronic terahertz systems dominate the recent literature, field-deployable terahertz technologies for rugged, compact, and ultimately low-cost screening and sensing will be based on electronics," said van der Weide.

According to van der Weide, the University of Wisconsin system is more practical than an optical or electro-optic system and can be scaled to the chip level. In addition, the wavelengths can be treated quasi-optically the same way laser-based systems work, which is of particular interest for field-deployable applications.

"We are looking for distinct reflections as a function of frequency and spectral signatures that indicate the presence of concealed threats," van der Weide said. "We have performed spectroscopy on plastic explosives, which is of extreme interest to the aviation industry, and bioagents such as anthrax." His group is also targeting the 0.1- to 0.6-THz portion of the spectrum for remote sensing.

The ESA-sponsored StarTiger program also focused on non-electro-optic terahertz technologies. More important, the StarTiger team achieved something no one in the terahertz community had done before: they built a compact, low-cost terahertz imager in just four months, using manufacturing techniques adapted from the semiconductor industry. The system was completed last October and has captured the first terahertz picture of a human hand (see Fig. 3).

FIGURE 3. ESA-sponsored StarTiger terahertz imager, built in just four months using manufacturing techniques adapted from the silicon industry, was completed last October and has captured the first terahertz picture of a human hand.

Click here to enlarge image

The imager built by the StarTiger team operates at 0.25 and 0.3 THz and uses heterodyne detection to create two-color images with contrast between materials with different transmission and reflection properties. One of the main advantages of the StarTiger imager is that it does not emit any radiation; it is a passive camera capturing pictures of the natural T-rays emitted by almost everything. In addition, the StarTiger team developed new technologies that should further advance the creation and fabrication of terahertz devices, including a two-color micromachined waveguide array the size of a postage stamp, a photonic bandgap mixer, and a micro-machined room-temperature detector.

"Terahertz technology is evolving quickly, and current electro-optical terahertz systems with a laser are on the order of a few hundred thousand dollars and weigh about 50 kg or less," said Robert Osiander of the Applied Physics Laboratory at Johns Hopkins University (Baltimore, MD, USA), which is using funding from an Army Research Office multi-university research initiative to investigate optical terahertz spectroscopy for trace-explosives detection. "The parallel development of electronic sources will make terahertz less expensive and much smaller, because they can be developed for the frequency range of interest." ..

KATHY KINCADE is contributing editor, Laser Focus World, a PennWell publication, www.laserfocus.com.

Company Info

AT&T Bell Labs www.bell-labs.com
Brookhaven National Laboratory www.bnl.gov
Delft University of Technology www.tudelft.nl
European Space Agency (ESA) www.esa.int
Jefferson Lab www.jlab.org
Johns Hopkins University www.jhu.edu
Lawrence Berkeley National Laboratory www.lbl.gov
Lockheed Martin Space Systems www.lockheedmartin.com
National Aeronautical and Space Administration www.nasa.gov
Picometrix www.picometrix.com
Rensselaer Polytechnic Institute (RPI) www.rpi.edu
TeraView www.teraview.co.uk
University of California, Santa Barbara (UCSB) www.ucsb.edu
University of Wisconsin www.wisc.edu

T-rays check shuttle foam

Researchers at Rensselaer Polytechnic Institute (RPI; Troy, NY, USA) and Lockheed Martin Space Systems (New Orleans, LA, USA) are investigating terahertz imaging as a potential nondestructive method for preflight inspection of the foam that is applied to space-shuttle fuel tanks. NASA (Washington, DC, USA) investigators believe that the

Columbia space-shuttle crash may have been caused by foam insulation breaking away and striking the left wing of the craft. So fuel-tank manufacturer Lockheed Martin asked X.-C. Zhang, the J. Erik Jonsson Professor of Science at RPI, to study a specially prepared sample of the foam material.

Researchers Xie Xu (left) and Hua Zhong (right) use a terahertz-imaging technique developed at Rensselaer Polytechnic Institute to successfully locate embedded defects in foam samples provided by Lockheed Martin Space Systems.

Click here to enlarge image

The sample was composed of material identical to the foam that is normally applied to the shuttle fuel tank, but instead of the continuous layer of foam normally applied to the tank, the sample consisted of a 2 × 2-ft block approximately 4 in. thick. An aluminum plate served as the base for two different insulating materials: a 1-in. layer of dense, corklike super-lightweight ablator (SLA) was applied on top of a 3-in. layer of closed-cell sprayed-on foam insulation (SOFI).

Eight man-made defects were scattered throughout the sample. The embedded imperfections mimicked defects that might occur in a normally produced foam application on the fuel tank. The two types of defects hidden in the sample were voids (air bubbles), ranging from 1/4 to 1 in., and debonds (separations between layers of foam or between a foam layer and the base).

Zhang's research team successfully used terahertz radiation to detect the embedded defects. The SLA and SOFI materials making up the insulating-foam sample are excellent subjects for terahertz radiation, according to Zhang. "The foam has a lower attenuation, allowing the terahertz waves to penetrate to a depth of many inches," he says.

The researchers used an 800-nm femtosecond laser with a 250-ns pulsewidth and 250-kHz repetition rate to generate the terahertz signal and a zinc telluride electro-optic crystal to detect it. They were able to locate and identify defects in the insulating-foam sample by measuring the signal amplitude, temporal delay, and waveform distortion of the signal. But the sample also posed unique challenges due to reflections from different layers of the foam, according to researcher Hua Zhong.

"Because we are playing in a refractory geometry, signal collection becomes an issue, and diffusion of the terahertz beam on passing through the foam significantly lowers collection efficiency," she says. To compensate for these factors, they placed the collection components on top of the testing platform and situated the mirrors to ensure that beams coming from different foam layers would be collected and overlap fairly well with the probe beam on the sensor crystal.

The next hurdle for the team is to boost the signal-to-noise ratio, which will also increase the scanning speed, added Zhong. "Right now it takes half a day to scan a 2 × 2-ft piece of foam. We could speed it up considerably, to one hour or less, by increasing the sensor crystal size to 40 × 40 cm and using a CCD camera," Zhong said.

HASSAUN JONES-BEY, editor, Laser Focus World; www.laserfocus.com.

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